Vacuum melting of compressed powders and hot rolling of the as-cast Ti-48Al-2Nb-0.7Cr-0.3Si intermetallic alloy : mechanical properties and microstructural analysis

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Authors

Ellard, John Jimmy Masache
Mathabathe, M.N.
Siyasiya, Charles Witness
Bolokang, A.S.

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Elsevier

Abstract

The amalgamated effect of hot-rolling, rapid cooling and heat treatment on the grain refinement and the resultant mechanical properties of an intermetallic sheet of nominal composition Ti-48Al-2Nb-0.7Cr-0.3Si was investigated. The sheet of 4 mm thickness was fabricated by hot-pack rolling from the vacuum arc remelted (VAR) ingot using a conventional two-high rolling mill. After the final rolling pass, the canned specimen was rapidly cooled in the air to room temperature followed by heat treatment in the α + γ region. The scanning electron microscopy (SEM) micrographs of the as-rolled sheet revealed slightly elongated grains of a typical “duplex (DP)” microstructure with a mean grain size of about 3 μm which grew to about 4 μm and became more equiaxed and homogeneous after heat treatment. Moreover, the EBSD micro-texture indicated a weak cube texture in the rolled + heat-treated sheet. Furthermore, the results from the profilometry-based indentation plastometry of the rolled + heat treated specimen illustrated the balanced and improved mechanical properties compared to the as-cast and as-rolled samples, and also those of similar alloy systems found in the literature.

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Keywords

Microstructural refinement, Hot-pack rolling, Intermetallic, γ-TiAl alloy, Vacuum arc remelted (VAR), Scanning electron microscopy (SEM), Electron backscattered diffraction (EBSD)

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Citation

Ellard, J.J.M., Mathabathe, M.N., Siyasiya, C. et al. 2023, 'Vacuum melting of compressed powders and hot rolling of the as-cast Ti-48Al-2Nb-0.7Cr-0.3Si intermetallic alloy: mechanical properties and microstructural analysis', Journal of Manufacturing Processes, vol. 101, pp. 1214-1223, doi : 10.1016/j.jmapro.2023.06.060.